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2019 The effect of cyclic intercritical annealing on microstructure of dual

Advanced High Strength Steels (AHSS) grades are currently the fastest growing materials in the automotive industry. AHSS offer a great potential for the development of automobile bodies with their mechanical properties of high formability and strength. Dual phase (DP) steels are increasingly popular AHSS grade in the automotive industry due to the excellent combination of high strength and good formability. The intercritical annealing of DP steel is generally two-stage heat treatment. DP steel sheet is annealed in the intercritical temperature range to produce ferrite and austenite and followed by accelerated cooling to transform the austenite phase to martensite. This study aims to examine effect of a cyclic intercritical annealing below and above A1 temperature on DP steel microstructure with comparison to the conventional intercritical annealing. The specimens were conventional intercritically annealed at different temperatures between 720 °C and 760°C. In cyclic intercritical annealing experiments, the temperature is cycled between 630 °C and an intercritical annealing temperature without any isothermal holding. After the conventional and cyclic intercritical annealing, the samples were investigated using light microscope and scanning electron microscope. Experimental results showed that a refinement of martensite and ferrite dual phase microstructure compare to conventional intercritical annealing.

International Iron & Steel Symposium
UDCS

Ayşe Kavruk Oğuz Gürkan Bilir Özge Ararat Ahmet Efe Gezmişoğlu

284 212
Subject Area: Materials Science Broadcast Area: International Type: Oral Paper Language: English
2017 Determining Retained Austenite Quantity and Composition with Heat Treatment Parameters in SAE52100 Steels

Influence of different austenitization conditions on retained austenite quantity and composition investigated on SAE 52100 steel. SAE 52100 steels are being widely used as bearing component regarding to their hardness and wear resistance. Traditional production cycle includes hot rolling, spheroidization, cold rolling, quenching from two phase region and tempering steps. This cycle results with martensitic matrix and undissolved course carbides. Course carbides maintain adequate wear performance but due to course carbides providing appropriate nucleation sites for crack propagation and growth this structure shows poor fatigue behavior. Previous studies showed better carbide size and distribution with experimental two step hardening cycle. This cycle results with considerable increase at retained austenite fraction. It’s well known that mechanically unstable retained austenite improves fatigue resistance in this type of steel. Transformation retained austenite to martensite caused by deformation eliminates local stresses and retards crack propagation and growth. XRD studies are carried on to determining retained austenite quantity with various austenitizing conditions. Computational simulations with Thermo-Calc and Dictra are used for predicting carbon concentration gradient of austenite during austenitization which determines retained austenite fraction at the end. A good correlation between XRD data and simulation results was obtained.

International Iron & Steel Symposium
UDCS

Ersoy Erişir Oğuz Gürkan Bilir Ahmet Efe Gezmişoğlu

327 265
Subject Area: Materials Science Broadcast Area: International Type: Oral Paper Language: English
2017 Examination of Solid State Nitrogen Absorption for Production of Nickel Free Stainless Steel

Co-Cr and 316L are the commonly used alloys in biomedical industry. However, both 316L and mostly used Co-Cr alloys as F-562, L-605 contain large portions of Ni as alloying element. Ni may cause allergic and toxic impacts on human health. In recent years, N-alloyed Ni free stainless steels seemed as good candidate for replacing Ni contained metals. However, liquid steel has a limited N solubility at atmospheric pressure. Thus, high pressured melting techniques are required. In this study, N alloying of ferritic 430 stainless steel sheet was performed in solid state. Nitrogen absorption of stainless steel was performed in a furnace filled with nitrogen gas with atmospheric pressure at 1200°C. Solid state N absorption was applied in four different time periods as 4, 8, 12, 24 hours. Microstructure after absorption process was investigated by Scanning Electron Microscope and Light Microscope. Fully austenitic structure was observed in surface of specimens. However, duplex microstructure of ferrite and austenite was seen in the center of specimen. Vickers hardness was carried out to evaluate of phases. It was concluded that optimum microstructure is achieved by 4 hours of N absorption.

International Iron & Steel Symposium
UDCS

Oğuz Gürkan Bilir İsmail GÜVENİR Ersoy Erişir

253 188
Subject Area: Materials Science Broadcast Area: International Type: Oral Paper Language: English
2017 The Effect of Prior Austenite Grain Size on Microstructure of Medium Carbon Dual Phase Steels

Finer martensitic and ferritic microstructures are demanded to obtain high strength and toughness for dual phase steels. In this study, reducing of prior austenite grain size selected as an effective method to reduce the size of dual phase microstructure. The effect of prior austenite grain size on microstructure of medium carbon dual phase steel produced by intercritical annealing were investigated for different austenitizing conditions. Annealing experiments were performed to fully austenitizate the steel at different austenitizing temperatures (900, 950, 1000ᵒC) and times (5, 10, 15 min) and followed by quenching. Finally, as-quenched martensitic microstructures were intercritical annealed at 760ᵒC for 15 min to attain martensitic and ferritic dual phase steel. The microstructures were analyzed using light microscopy and image analysis methods. It is concluded that grain size of dual phase steel is reducing by decreasing of the austenitizing temperature and the holding time.

International Iron & Steel Symposium
UDCS

Ersoy Erişir Özge Ararat Oğuz Gürkan Bilir

278 232
Subject Area: Materials Science Broadcast Area: International Type: Oral Paper Language: English